ANALYTICAL REPORT
January 27, 2017
Gallatin Water Department
Sample Delivery Group:
L884462
Samples Received:
01/18/2017
Project Number:
2927B
Description:
Drinking Water - Inorganic Chemical Monitoring
Site:
0253
Report To:
Mr. David Kellogg
239 Hancock Street
Gallatin, TN 37066
Entire Report Reviewed By:
January 27, 2017
[Preliminary Report]
Rodney Shinbaum
Technical Service Representative
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
January 27, 2017
Rodney Shinbaum
Technical Service Representative
ONE LAB. NATIONWIDE.
TABLE OF CONTENTS
¹Cp: Cover Page
1
²Tc: Table of Contents
2
³Ss: Sample Summary
3
⁴Cn: Case Narrative
4
⁵Sr: Sample Results
5
RAW WATER L884462-01
5
⁶Qc: Quality Control Summary
7
Gravimetric Analysis by Method 2540 C-1997
7
Wet Chemistry by Method 2120B
8
Wet Chemistry by Method 2150 B-2011
9
Wet Chemistry by Method 300.0
10
Wet Chemistry by Method 335.4
12
Wet Chemistry by Method 5540 C-2000
13
Mercury by Method 245.1
14
Metals (ICP) by Method 200.7
15
Metals (ICPMS) by Method 200.8
17
⁷Gl: Glossary of Terms
19
⁸Al: Accreditations & Locations
20
⁹Sc: Chain of Custody
21
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SAMPLE SUMMARY
Collected by Collected date/time
Received date/time
RAW WATER L884462-01 DW
T. Everett 01/18/17 10:15 01/18/17 11:05
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Gravimetric Analysis by Method 2540 C-1997 WG944938 1 01/22/17 03:39 01/22/17 07:22 JM
Mercury by Method 245.1 WG946060 1 01/24/17 12:14 01/24/17 19:25 NJB
Metals (ICP) by Method 200.7 WG944806 1 01/21/17 08:47 01/23/17 13:13 CCE
Metals (ICPMS) by Method 200.8 WG944521 1 01/21/17 08:53 01/23/17 22:00 VSS
Metals (ICPMS) by Method 200.8 WG944521 1 01/21/17 08:53 01/24/17 11:42 LAT
Wet Chemistry by Method 2120B WG944415 1 01/20/17 09:47 01/20/17 09:47 MHM
Wet Chemistry by Method 2150 B-2011 WG944414 1 01/18/17 17:12 01/18/17 17:12 MHM
Wet Chemistry by Method 300.0 WG944511 1 01/20/17 02:25 01/20/17 02:25 KCF
Wet Chemistry by Method 335.4 WG946724 1 01/25/17 22:16 01/26/17 18:18 ASK
Wet Chemistry by Method 5540 C-2000 WG944757 .25 01/20/17 07:30 01/20/17 08:27 MHM
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Rodney Shinbaum
Technical Service Representative
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SAMPLE RESULTS - 01
L884462
RAW WATER
Collected date/time: 01/18/17 10:15
Additional Information
Result Units Reference Limit
Analyte
pH (On Site) 7.4
Entry Point A
Sample Type S
Gravimetric Analysis by Method 2540 C-1997
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Dissolved Solids 127 10.0 500 1 01/22/2017 07:22 WG944938 JM
Wet Chemistry by Method 2120B
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte pcu pcu pcu date / time
Color 20.0 1.00 15 1 01/20/2017 09:47 WG944415 MHM
Wet Chemistry by Method 2150 B-2011
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte T.O.N. T.O.N. T.O.N. date / time
Odor 1.00 1.00 3 1 01/18/2017 17:12 WG944414 MHM
Wet Chemistry by Method 300.0
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Chloride 4.65 1.00 250 1 01/20/2017 02:25 WG944511 KCF
Fluoride ND 0.100 2 1 01/20/2017 02:25 WG944511 KCF
Sulfate 20.0 5.00 250 1 01/20/2017 02:25 WG944511 KCF
Wet Chemistry by Method 335.4
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Cyanide ND 0.00500 0.20 1 01/26/2017 18:18 WG946724 ASK
Wet Chemistry by Method 5540 C-2000
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
MBAS ND 0.0250 0.50 .25 01/20/2017 08:27 WG944757 MHM
Mercury by Method 245.1
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Mercury ND 0.000200 0.0020 1 01/24/2017 19:25 WG946060 NJB
Metals (ICP) by Method 200.7
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Aluminum ND 0.200 0.20 1 01/23/2017 13:13 WG944806 CCE
Barium 0.0240 0.00500 2 1 01/23/2017 13:13 WG944806 CCE
Chromium ND 0.0100 0.10 1 01/23/2017 13:13 WG944806 CCE
Copper 0.0445 0.0100 1 1 01/23/2017 13:13 WG944806 CCE
Iron 0.147 0.100 0.30 1 01/23/2017 13:13 WG944806 CCE
Manganese 0.0386 0.0100 0.05 1 01/23/2017 13:13 WG944806 CCE
Nickel ND 0.0100 0.10 1 01/23/2017 13:13 WG944806 CCE
Silver ND 0.00500 0.10 1 01/23/2017 13:13 WG944806 CCE
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SAMPLE RESULTS - 01
L884462
RAW WATER
Collected date/time: 01/18/17 10:15
Metals (ICP) by Method 200.7
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Sodium 5.08 1.00 1 01/23/2017 13:13 WG944806 CCE
Zinc ND 0.0500 5 1 01/23/2017 13:13 WG944806 CCE
Metals (ICPMS) by Method 200.8
Result Qualifier Det. Limit Reference Limit Dilution Analysis Batch Analyst
Analyte mg/l mg/l mg/l date / time
Antimony ND 0.00100 0.0060 1 01/23/2017 22:00 WG944521 VSS
Arsenic ND 0.00100 0.01 1 01/24/2017 11:42 WG944521 LAT
Beryllium ND 0.00100 0.0040 1 01/23/2017 22:00 WG944521 VSS
Cadmium ND 0.00100 0.0050 1 01/23/2017 22:00 WG944521 VSS
Selenium ND 0.00100 0.05 1 01/24/2017 11:42 WG944521 LAT
Thallium ND 0.00100 0.0020 1 01/24/2017 11:42 WG944521 LAT
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QUALITY CONTROL SUMMARY
WG944938
Gravimetric Analysis by Method 2540 C-1997
L884462-01
Method Blank (MB)
(MB) R3192595-1 01/22/17 07:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U 2.82 10.0
L884458-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884458-01 01/22/17 07:22 • (DUP) R3192595-4 01/22/17 07:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Dissolved Solids 195 192 1 1.55 5
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3192595-2 01/22/17 07:22 • (LCSD) R3192595-3 01/22/17 07:22
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Dissolved Solids 8800 8260 8480 93.9 96.4 85.0-115 2.63 5
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QUALITY CONTROL SUMMARY
WG944415
Wet Chemistry by Method 2120B
L884462-01
L884458-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884458-01 01/20/17 09:47 • (DUP) WG944415-1 01/20/17 09:47
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte pcu pcu % %
Color 1.00 1.00 1 0.000 20
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QUALITY CONTROL SUMMARY
WG944414
Wet Chemistry by Method 2150 B-2011
L884462-01
Method Blank (MB)
(MB) WG944414-1 01/18/17 17:12
MB Result MB Qualifier MB MDL MB RDL
Analyte T.O.N. T.O.N. T.O.N.
Odor 1.00 0.333 1.00
L884458-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884458-01 01/18/17 17:12 • (DUP) WG944414-2 01/18/17 17:12
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte T.O.N. T.O.N. % %
Odor 1.00 1.00 1 0.000 20
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QUALITY CONTROL SUMMARY
WG944511
Wet Chemistry by Method 300.0
L884462-01
Method Blank (MB)
(MB) R3191795-1 01/19/17 17:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Chloride U 0.0519 1.00
Fluoride U 0.0099 0.100
Sulfate U 0.0774 5.00
L884477-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884477-01 01/19/17 21:12 • (DUP) R3191795-6 01/19/17 21:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Chloride 10.4 10.5 1 0 20
Fluoride 0.399 0.400 1 0 20
Sulfate 10.4 10.4 1 0 20
L884592-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884592-01 01/19/17 22:11 • (DUP) R3191795-7 01/19/17 23:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Chloride 28.4 28.5 1 0 20
Fluoride 0.214 0.202 1 6 20
Sulfate 32.2 32.3 1 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3191795-2 01/19/17 17:58 • (LCSD) R3191795-3 01/19/17 18:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Chloride 40.0 39.3 39.2 98 98 90-110 0 20
Fluoride 8.00 7.89 7.89 99 99 90-110 0 20
Sulfate 40.0 39.2 39.1 98 98 90-110 0 20
L884316-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L884316-02 01/19/17 18:57 • (MS) R3191795-5 01/19/17 19:12
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l % %
Fluoride 5.00 8.70 13.1 87 1 80-120 E
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QUALITY CONTROL SUMMARY
WG944511
Wet Chemistry by Method 300.0
L884462-01
L884601-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884601-01 01/20/17 00:55 • (MS) R3191795-8 01/20/17 01:10 • (MSD) R3191795-9 01/20/17 01:25
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Chloride 50.0 23.1 73.7 73.9 101 102 1 80-120 0 20
Fluoride 5.00 ND 5.12 5.18 102 104 1 80-120 1 20
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QUALITY CONTROL SUMMARY
WG946724
Wet Chemistry by Method 335.4
L884462-01
Method Blank (MB)
(MB) R3193100-1 01/26/17 18:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Cyanide U 0.0018 0.00500
L884958-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884958-01 01/26/17 18:24 • (DUP) R3193100-6 01/26/17 18:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Cyanide ND 0.00394 1 0 20
L885180-06 Original Sample (OS) • Duplicate (DUP)
(OS) L885180-06 01/26/17 18:36 • (DUP) R3193100-7 01/26/17 18:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
Cyanide ND 0.000 1 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193100-2 01/26/17 18:12 • (LCSD) R3193100-3 01/26/17 18:13
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Cyanide 0.100 0.106 0.108 106 108 90-110 2 20
L884893-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884893-02 01/26/17 18:19 • (MS) R3193100-4 01/26/17 18:20 • (MSD) R3193100-5 01/26/17 18:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Cyanide 0.200 ND 0.189 0.190 95 95 1 90-110 1 20
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Tc
3
Ss
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Cn
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QUALITY CONTROL SUMMARY
WG944757
Wet Chemistry by Method 5540 C-2000
L884462-01
Method Blank (MB)
(MB) R3191808-1 01/20/17 08:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
MBAS U 0.019 0.100
L884458-01 Original Sample (OS) • Duplicate (DUP)
(OS) L884458-01 01/20/17 08:26 • (DUP) R3191808-4 01/20/17 08:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l % %
MBAS ND 0.000 .25 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3191808-2 01/20/17 08:23 • (LCSD) R3191808-3 01/20/17 08:23
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
MBAS 1.00 0.929 0.909 93 91 90-110 2 20
L884767-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884767-02 01/20/17 08:29 • (MS) R3191808-5 01/20/17 08:30 • (MSD) R3191808-6 01/20/17 08:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
MBAS 1.00 U 0.946 0.961 95 96 1 90-110 2 20
1
Cp
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Tc
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QUALITY CONTROL SUMMARY
WG946060
Mercury by Method 245.1
L884462-01
Method Blank (MB)
(MB) R3192564-1 01/24/17 19:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000049 0.000200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3192564-2 01/24/17 19:04 • (LCSD) R3192564-3 01/24/17 19:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Mercury 0.00300 0.00297 0.00286 99 95 85-115 4 20
L884958-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884958-01 01/24/17 19:09 • (MS) R3192564-4 01/24/17 19:11 • (MSD) R3192564-5 01/24/17 19:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Mercury 0.00300 ND 0.00306 0.00310 102 103 1 70-130 1 20
1
Cp
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Tc
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Ss
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Cn
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QUALITY CONTROL SUMMARY
WG944806
Metals (ICP) by Method 200.7
L884462-01
Method Blank (MB)
(MB) R3192216-1 01/23/17 12:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Aluminum 0.0292 J 0.0273 0.200
Barium U 0.001 0.00500
Chromium U 0.0018 0.0100
Copper U 0.007 0.0100
Iron U 0.0282 0.100
Manganese U 0.002 0.0100
Nickel U 0.0058 0.0100
Silver U 0.0027 0.00500
Sodium U 0.0939 1.00
Zinc U 0.0034 0.0500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3192216-3 01/23/17 12:54 • (LCSD) R3192216-4 01/23/17 12:56
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Aluminum 10.0 10.3 10.2 103 102 85-115 1 20
Barium 1.00 1.05 1.03 105 103 85-115 1 20
Chromium 1.00 1.03 1.01 103 101 85-115 3 20
Copper 1.00 1.02 0.998 102 100 85-115 2 20
Iron 10.0 10.1 9.92 101 99 85-115 2 20
Manganese 1.00 0.992 0.977 99 98 85-115 1 20
Nickel 1.00 1.04 1.03 104 103 85-115 1 20
Silver 0.200 0.197 0.194 99 97 85-115 2 20
Sodium 10.0 10.1 9.93 101 99 85-115 2 20
Zinc 1.00 1.06 1.04 106 104 85-115 1 20
L884458-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884458-01 01/23/17 12:59 • (MS) R3192216-6 01/23/17 13:05 • (MSD) R3192216-7 01/23/17 13:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Aluminum 10.0 ND 10.2 10.8 102 108 1 75-125 6 20
Barium 1.00 0.0211 1.05 1.11 103 109 1 75-125 6 20
Chromium 1.00 ND 1.01 1.07 101 107 1 75-125 5 20
Copper 1.00 ND 1.00 1.06 100 106 1 75-125 6 20
Iron 10.0 ND 9.91 10.5 99 105 1 75-125 6 20
Manganese 1.00 ND 0.971 1.02 97 102 1 75-125 5 20
Nickel 1.00 ND 1.03 1.09 103 109 1 75-125 6 20
1
Cp
2
Tc
3
Ss
4
Cn
5
Sr
6
Qc
7
Gl
8
Al
9
Sc
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ONE LAB. NATIONWIDE.
QUALITY CONTROL SUMMARY
WG944806
Metals (ICP) by Method 200.7
L884462-01
L884458-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884458-01 01/23/17 12:59 • (MS) R3192216-6 01/23/17 13:05 • (MSD) R3192216-7 01/23/17 13:07
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Silver 0.200 ND 0.195 0.205 97 103 1 75-125 5 20
Sodium 10.0 10.6 20.7 22.6 101 120 1 75-125 9 20
Zinc 1.00 ND 1.04 1.09 104 109 1 75-125 5 20
1
Cp
2
Tc
3
Ss
4
Cn
5
Sr
6
Qc
7
Gl
8
Al
9
Sc
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ONE LAB. NATIONWIDE.
QUALITY CONTROL SUMMARY
WG944521
Metals (ICPMS) by Method 200.8
L884462-01
Method Blank (MB)
(MB) R3192306-1 01/23/17 19:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00100
Beryllium U 0.00028 0.00100
Cadmium U 0.00022 0.00100
Method Blank (MB)
(MB) R3192467-1 01/24/17 11:14
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Arsenic U 0.00017 0.00100
Selenium U 0.00032 0.00100
Thallium U 0.00028 0.00100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3192306-3 01/23/17 19:59 • (LCSD) R3192306-4 01/23/17 20:05
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Antimony 0.0579 0.0518 0.0516 89 89 85-115 0 20
Beryllium 0.0500 0.0477 0.0538 95 108 85-115 12 20
Cadmium 0.0500 0.0488 0.0473 98 95 85-115 3 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3192467-3 01/24/17 11:21 • (LCSD) R3192467-4 01/24/17 11:24
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % % % %
Arsenic 0.0500 0.0485 0.0477 97 95 85-115 2 20
Selenium 0.0500 0.0501 0.0496 100 99 85-115 1 20
Thallium 0.0500 0.0456 0.0481 91 96 85-115 5 20
L884190-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884190-01 01/23/17 20:10 • (MS) R3192306-5 01/23/17 20:16 • (MSD) R3192306-6 01/23/17 20:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Antimony 0.0500 ND 0.0531 0.0514 106 103 1 70-130 3 20
Beryllium 0.0500 ND 0.0426 0.0451 85 90 1 70-130 6 20
1
Cp
2
Tc
3
Ss
4
Cn
5
Sr
6
Qc
7
Gl
8
Al
9
Sc
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ONE LAB. NATIONWIDE.
QUALITY CONTROL SUMMARY
WG944521
Metals (ICPMS) by Method 200.8
L884462-01
L884190-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L884190-01 01/23/17 20:10 • (MS) R3192306-5 01/23/17 20:16 • (MSD) R3192306-6 01/23/17 20:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Cadmium 0.0500 ND 0.0472 0.0466 94 93 1 70-130 1 20
1
Cp
2
Tc
3
Ss
4
Cn
5
Sr
6
Qc
7
Gl
8
Al
9
Sc
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ONE LAB. NATIONWIDE.
GLOSSARY OF TERMS
Abbreviations and Definitions
SDG
Sample Delivery Group.
MDL
Method Detection Limit.
RDL
Reported Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
U
Not detected at the Reporting Limit (or MDL where applicable).
RPD
Relative Percent Difference.
Original Sample
The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
Rec.
Recovery.
Qualifier
Description
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument
established by the initial calibration (ICAL).
J
The identification of the analyte is acceptable; the reported value is an estimate.
1
Cp
2
Tc
3
Ss
4
Cn
5
Sr
6
Qc
7
Gl
8
Al
9
Sc
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ONE LAB. NATIONWIDE.
ACCREDITATIONS & LOCATIONS
1
Cp
2
Tc
3
Ss
4
Cn
5
Sr
6
Qc
7
Gl
8
Al
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Sc
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ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
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ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support oces, please
contact our main oce. ESC Lab Sciences performs all testing at our central laboratory.
1.
Drinking Water
2.
Underground Storage Tanks
3.
Aquatic Toxicity
4.
Chemical/Microbiological
5.
Mold
n/a
Accreditation not applicable
1461.02A2LA – ISO 17025
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* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
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